Codeofchina.com is in charge of this English translation. In case of any doubt about the English translation, the Chinese original shall be considered authoritative.
This standard is developed in accordance with the rules given in GB/T 1.1-2009.
This standard supersedes GB/T 19541-2004 Soybean Meal (Solvent) for Feedstuff. In addition to editorial changes, the following technical changes have been made with respect to GB/T 19541-2004:
——the standard title is revised as Feed Materials—Soybean Meal;
——'Scope' is modified (see Chapter 1);
——'Normative References' is modified (see Chapter 2);
——in sensory properties, fawn and caking is deleted, while maple or sorrel and coarse particle type are added (see 4.1);
——the inclusion indexes are deleted (see 4.2 of Edition 2004);
——the quality grade indexes are modified (see 4.2);
——the net content requirements are added (see 4.4);
——the inclusion inspection is deleted (see 5.1 of Edition 2004);
——the inspection of sensory properties and urease activity is modified (see 5.1 and 5.7);
——the inspection of lysine, hygienic index and net content is added (see 5.6, 5.9 and 5.10);
——the method for determination of protein solubility in potassium-hydroxide solution is adjusted to Annex A (see 5.8);
——the permissible errors in test method and monitoring and arbitration requirements are deleted (see 5.8 and 5.9 of Edition 2004);
——the inspection rules are modified (see Chapter 6);
——the soybean meal produced with transgenic soybean is added which shall be in accordance with the requirements of Measures for Management of Labelling for Agricultural Genetically Modified Organisms (see 7.1);
——the determination of protein solubility in potassium-hydroxide solution is modified (see Annex A).
This standard was proposed by and is under the jurisdiction of the National Technical Committee on Feed Industry of Standardization Administration of China (SAC/TC 76).
The previous editions of the standard superseded by this standard are as follows:
——GB/T 10380-1989, GB/T 19541-2004.
Feed Materials—Soybean Meal
1 Scope
This standard specifies the relevant terms and definitions, requirements, test methods, inspection rules, labelling, packaging, transportation and storage of soybean meal for feed materials.
This standard is applicable to soybean meal for feed materials produced with soybean after oil extraction by prepressing extraction or direct solvent extraction, or with soybean cake after oil extraction, or with soybean germ after oil extraction by expansion extraction.
2 Normative References
The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies.
GB/T 6432 Method for the Determination of Crude Protein in Feedstuffs
GB/T 6434 Feeding Stuffs―Determination of Crude Fiber Content Method with Intermediate Filtration
GB/T 6435 Determination of Moisture in Feeds
GB/T 6438 Animal Feeding Stuffs—Determination of Crude Ash
GB/T 6682 Water for Analytical Laboratory Use—Specification and Test Methods
GB/T 8622 Determination of Urease Activity in Soya Bean Products for Feeds
GB 10648 Feed Label
GB 13078 Hygienical Standard for Feeds
GB/T 14698-2002 Test Method of Feed Microscopy
GB/T 14699.1 Animal Feeding Stuffs—Sampling
GB/T 18246 Determination of Amino Acids in Feeds
GB/T 18823 Permitted Tolerants for Judgement of Testing Results in Feeds
GB/T 20195 Animal Feeding Stuffs—Preparation of Test Samples
JJF 1070 Rules of Metrological Testing for Net Quantity of Products in Prepackages with Fixed Content
Measures for the Metrological Supervision and Administration of Products in Prepackages with Fixed Content (AQSIQ Decree [2005] No.75)
3 Term and Definition
For the purposes of this document, the following term and definition apply.
3.1
protein solubility in potassium-hydroxide solution
mass fraction of crude protein content soluble in 0.2% potassium-hydroxide solution in the total crude protein content in soybean meal sample under the conditions as given in Annex A
4 Requirements
4.1 Sensory Properties
This product is pale yellow, maple or sorrel and appears as irregular fragment, coarse particle or coarse powder, without fermentation, mould, insect pest, peculiar smell or foreign odor.
4.2 Quality grade indexes
See Table 1 for quality grade indexes.
Table 1 Quality Grade Indexes
Item Grade
Special I II III
Crude protein /% ≥48.0 ≥46.0 ≥43.0 ≥41.0
Crude fiber /% ≤5.0 ≤7.0 ≤7.0 ≤7.0
Lysine /% ≥2.50 ≥2.30
Moisture content /% ≤12.5
Crude ash /% ≤7.0
Urease activity /(U/g) ≤0.30
Protein solubility in potassium-hydroxide solution a/% ≥73.0
a The index of soybean meal for feeds produced with soybean cake after oil extraction is stipulated by the supplier and the demander.
4.3 Hygienic index
It shall comply with GB 13078.
4.4 Net content
It shall be subject to the label and the deviation shall comply with those specified in Measures for the Metrological Supervision and Administration of Products in Prepackages with Fixed Content.
5 Test Methods
5.1 Sensory properties
It shall be in accordance with Chapter 7 of GB/T 14698-2002.
5.2 Crude protein
It shall be in accordance with GB/T 6432.
5.3 Crude fiber
It shall be in accordance with GB/T 6434.
5.4 Moisture content
It shall be in accordance with GB/T 6435.
5.5 Crude ash
It shall be in accordance with GB/T 6438.
5.6 Lysine
It shall be in accordance with GB/T 18246.
5.7 Urease activity
It shall be in accordance with GB/T 8622.
5.8 Protein solubility in potassium-hydroxide solution
It shall be in accordance with Annex A.
5.9 Hygienic index
It shall be in accordance with GB 13078.
5.10 Net content
It shall be in accordance with JJF 1070.
6 Inspection Rules
6.1 Batching
Products which are of the same specification and produced continuously with the same batch of materials in the same process on the same date of production are considered as a batch.
6.2 Sampling
It shall be in accordance with GB/T 14699.1.
6.3 Delivery inspection
Sensory properties, moisture content, crude protein and urease activity are included in the delivery inspection items.
6.4 Type inspection
Type inspection shall be carried out in any of the following cases and the inspection items are those specified in this standard:
a) Where materials, process or design changes greatly after formal production;
b) Type inspection is carried out once every half year after formal production;
c) Production is resumed after shutdown for more than 3 months;
d) Where the result of delivery inspection is greatly different from the previous type inspection result;
e) Where the product quality supervision department proposes the requirements for type inspection.
Foreword i
1 Scope
2 Normative References
3 Term and Definition
4 Requirements
5 Test Methods
6 Inspection Rules
7 Labelling, Packaging, Transportation and Storage
Annex A (Normative) Determination of Protein Solubility in Potassium-Hydroxide Solution
Codeofchina.com is in charge of this English translation. In case of any doubt about the English translation, the Chinese original shall be considered authoritative.
This standard is developed in accordance with the rules given in GB/T 1.1-2009.
This standard supersedes GB/T 19541-2004 Soybean Meal (Solvent) for Feedstuff. In addition to editorial changes, the following technical changes have been made with respect to GB/T 19541-2004:
——the standard title is revised as Feed Materials—Soybean Meal;
——'Scope' is modified (see Chapter 1);
——'Normative References' is modified (see Chapter 2);
——in sensory properties, fawn and caking is deleted, while maple or sorrel and coarse particle type are added (see 4.1);
——the inclusion indexes are deleted (see 4.2 of Edition 2004);
——the quality grade indexes are modified (see 4.2);
——the net content requirements are added (see 4.4);
——the inclusion inspection is deleted (see 5.1 of Edition 2004);
——the inspection of sensory properties and urease activity is modified (see 5.1 and 5.7);
——the inspection of lysine, hygienic index and net content is added (see 5.6, 5.9 and 5.10);
——the method for determination of protein solubility in potassium-hydroxide solution is adjusted to Annex A (see 5.8);
——the permissible errors in test method and monitoring and arbitration requirements are deleted (see 5.8 and 5.9 of Edition 2004);
——the inspection rules are modified (see Chapter 6);
——the soybean meal produced with transgenic soybean is added which shall be in accordance with the requirements of Measures for Management of Labelling for Agricultural Genetically Modified Organisms (see 7.1);
——the determination of protein solubility in potassium-hydroxide solution is modified (see Annex A).
This standard was proposed by and is under the jurisdiction of the National Technical Committee on Feed Industry of Standardization Administration of China (SAC/TC 76).
The previous editions of the standard superseded by this standard are as follows:
——GB/T 10380-1989, GB/T 19541-2004.
Feed Materials—Soybean Meal
1 Scope
This standard specifies the relevant terms and definitions, requirements, test methods, inspection rules, labelling, packaging, transportation and storage of soybean meal for feed materials.
This standard is applicable to soybean meal for feed materials produced with soybean after oil extraction by prepressing extraction or direct solvent extraction, or with soybean cake after oil extraction, or with soybean germ after oil extraction by expansion extraction.
2 Normative References
The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies.
GB/T 6432 Method for the Determination of Crude Protein in Feedstuffs
GB/T 6434 Feeding Stuffs―Determination of Crude Fiber Content Method with Intermediate Filtration
GB/T 6435 Determination of Moisture in Feeds
GB/T 6438 Animal Feeding Stuffs—Determination of Crude Ash
GB/T 6682 Water for Analytical Laboratory Use—Specification and Test Methods
GB/T 8622 Determination of Urease Activity in Soya Bean Products for Feeds
GB 10648 Feed Label
GB 13078 Hygienical Standard for Feeds
GB/T 14698-2002 Test Method of Feed Microscopy
GB/T 14699.1 Animal Feeding Stuffs—Sampling
GB/T 18246 Determination of Amino Acids in Feeds
GB/T 18823 Permitted Tolerants for Judgement of Testing Results in Feeds
GB/T 20195 Animal Feeding Stuffs—Preparation of Test Samples
JJF 1070 Rules of Metrological Testing for Net Quantity of Products in Prepackages with Fixed Content
Measures for the Metrological Supervision and Administration of Products in Prepackages with Fixed Content (AQSIQ Decree [2005] No.75)
3 Term and Definition
For the purposes of this document, the following term and definition apply.
3.1
protein solubility in potassium-hydroxide solution
mass fraction of crude protein content soluble in 0.2% potassium-hydroxide solution in the total crude protein content in soybean meal sample under the conditions as given in Annex A
4 Requirements
4.1 Sensory Properties
This product is pale yellow, maple or sorrel and appears as irregular fragment, coarse particle or coarse powder, without fermentation, mould, insect pest, peculiar smell or foreign odor.
4.2 Quality grade indexes
See Table 1 for quality grade indexes.
Table 1 Quality Grade Indexes
Item Grade
Special I II III
Crude protein /% ≥48.0 ≥46.0 ≥43.0 ≥41.0
Crude fiber /% ≤5.0 ≤7.0 ≤7.0 ≤7.0
Lysine /% ≥2.50 ≥2.30
Moisture content /% ≤12.5
Crude ash /% ≤7.0
Urease activity /(U/g) ≤0.30
Protein solubility in potassium-hydroxide solution a/% ≥73.0
a The index of soybean meal for feeds produced with soybean cake after oil extraction is stipulated by the supplier and the demander.
4.3 Hygienic index
It shall comply with GB 13078.
4.4 Net content
It shall be subject to the label and the deviation shall comply with those specified in Measures for the Metrological Supervision and Administration of Products in Prepackages with Fixed Content.
5 Test Methods
5.1 Sensory properties
It shall be in accordance with Chapter 7 of GB/T 14698-2002.
5.2 Crude protein
It shall be in accordance with GB/T 6432.
5.3 Crude fiber
It shall be in accordance with GB/T 6434.
5.4 Moisture content
It shall be in accordance with GB/T 6435.
5.5 Crude ash
It shall be in accordance with GB/T 6438.
5.6 Lysine
It shall be in accordance with GB/T 18246.
5.7 Urease activity
It shall be in accordance with GB/T 8622.
5.8 Protein solubility in potassium-hydroxide solution
It shall be in accordance with Annex A.
5.9 Hygienic index
It shall be in accordance with GB 13078.
5.10 Net content
It shall be in accordance with JJF 1070.
6 Inspection Rules
6.1 Batching
Products which are of the same specification and produced continuously with the same batch of materials in the same process on the same date of production are considered as a batch.
6.2 Sampling
It shall be in accordance with GB/T 14699.1.
6.3 Delivery inspection
Sensory properties, moisture content, crude protein and urease activity are included in the delivery inspection items.
6.4 Type inspection
Type inspection shall be carried out in any of the following cases and the inspection items are those specified in this standard:
a) Where materials, process or design changes greatly after formal production;
b) Type inspection is carried out once every half year after formal production;
c) Production is resumed after shutdown for more than 3 months;
d) Where the result of delivery inspection is greatly different from the previous type inspection result;
e) Where the product quality supervision department proposes the requirements for type inspection.
Contents of GB/T 19541-2017
Foreword i
1 Scope
2 Normative References
3 Term and Definition
4 Requirements
5 Test Methods
6 Inspection Rules
7 Labelling, Packaging, Transportation and Storage
Annex A (Normative) Determination of Protein Solubility in Potassium-Hydroxide Solution
