1 Scope
This Standard specifies liquid chromatography - tandem mass spectrometric determination method of chloramphenicol residues in milk.
This Standard is applicable to the determination of residue content of chloramphenicol in milk.
2 Normative References
The following normative documents contain provisions which, through reference in this Standard, constitute provisions of this Standard. For dated references, subsequent amendments (excluding corrigendum contents) to, or revisions of, any of these publications do not apply. However, all parties coming to an agreement according to this Standard are encouraged to study whether the latest editions of these documents are applicable. For undated references, the latest editions of the normative references apply.
GB/T 1.1-2000 Directives for Standardization - Part 1: Rules for the Structure and Drafting of Standards
GB/T 6682-1992 Water for Analytical Laboratory Use - Specification and Test Methods
3 Principle
Contents
Foreword
1 Scope
2 Normative References
3 Principle
4 Reagents and Materials
5 Apparatus and Equipment
6 Preparation and Storage of Specimen
6.1 Specimen Preparation
6.2 Specimen Storage
7 Determination Procedures
7.1 Extraction
7.2 Purification
7.3 Preparation of Standard Curve
7.4 Determination
7.5 Blank Test
8 Result Calculation and Expression
9 Sensitivity, Accuracy and Precision of Detection Method
9.1 Sensitivity
9.2 Accuracy
9.3 Precision
Appendix A (Informative)
1 Scope
This Standard specifies liquid chromatography - tandem mass spectrometric determination method of chloramphenicol residues in milk.
This Standard is applicable to the determination of residue content of chloramphenicol in milk.
2 Normative References
The following normative documents contain provisions which, through reference in this Standard, constitute provisions of this Standard. For dated references, subsequent amendments (excluding corrigendum contents) to, or revisions of, any of these publications do not apply. However, all parties coming to an agreement according to this Standard are encouraged to study whether the latest editions of these documents are applicable. For undated references, the latest editions of the normative references apply.
GB/T 1.1-2000 Directives for Standardization - Part 1: Rules for the Structure and Drafting of Standards
GB/T 6682-1992 Water for Analytical Laboratory Use - Specification and Test Methods
3 Principle
Contents of GB/T 29668-2013
Contents
Foreword
1 Scope
2 Normative References
3 Principle
4 Reagents and Materials
5 Apparatus and Equipment
6 Preparation and Storage of Specimen
6.1 Specimen Preparation
6.2 Specimen Storage
7 Determination Procedures
7.1 Extraction
7.2 Purification
7.3 Preparation of Standard Curve
7.4 Determination
7.5 Blank Test
8 Result Calculation and Expression
9 Sensitivity, Accuracy and Precision of Detection Method
9.1 Sensitivity
9.2 Accuracy
9.3 Precision
Appendix A (Informative)
