Textiles - Determination of phosphate compounds
WARNING - Persons using this document shall be familiar with normal laboratory practice. This document does not purport to address all of the safety problems. It is the responsibility of the user to establish appropriate safety and health practices and to ensure compliance with any national regulatory conditions.
1 Scope
This document describes the gas chromatography and gas chromatography-mass spectrometry (GC-MS) methods for the determination of the content of eight phosphate compounds in textiles.
This document is applicable to all kinds of textiles.
2 Normative references
No normative reference is listed in this document.
3 Terms and definitions
No terms and definitions are listed in this document.
4 Principle
The specimens are extracted ultrasonically with ethyl acetate, and after being filtered by membrane, the extract solutions will be determined by a gas chromatograph equipped with a flame photometric detector (P-type), or determined by gas chromatograph-mass spectrometer and quantified by external standard method.
Foreword I
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents and materials
6 Apparatus
7 Analytical procedure
8 Calculation and expression of results
9 Limit of quantification and precision
10 Test report
Annex A (Informative) The gas chromatogram for standard substances of phosphate compounds
Annex B (Informative) The GC-MS selected ion chromatogram for standard substances of phosphate compounds
Standard
GB/T 42696-2023 Textiles—Determination of phosphate compounds (English Version)
Textiles - Determination of phosphate compounds
WARNING - Persons using this document shall be familiar with normal laboratory practice. This document does not purport to address all of the safety problems. It is the responsibility of the user to establish appropriate safety and health practices and to ensure compliance with any national regulatory conditions.
1 Scope
This document describes the gas chromatography and gas chromatography-mass spectrometry (GC-MS) methods for the determination of the content of eight phosphate compounds in textiles.
This document is applicable to all kinds of textiles.
2 Normative references
No normative reference is listed in this document.
3 Terms and definitions
No terms and definitions are listed in this document.
4 Principle
The specimens are extracted ultrasonically with ethyl acetate, and after being filtered by membrane, the extract solutions will be determined by a gas chromatograph equipped with a flame photometric detector (P-type), or determined by gas chromatograph-mass spectrometer and quantified by external standard method.
Contents of GB/T 42696-2023
Foreword I
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents and materials
6 Apparatus
7 Analytical procedure
8 Calculation and expression of results
9 Limit of quantification and precision
10 Test report
Annex A (Informative) The gas chromatogram for standard substances of phosphate compounds
Annex B (Informative) The GC-MS selected ion chromatogram for standard substances of phosphate compounds
