Dentistry - Testing of adhesion to tooth structure
1 Scope
This document specifies two bond strength measurements tests (tensile and shear), test for measurement of marginal gaps around fillings, a microleakage test, and some specific test methods for bond strength measurements.
This document gives guidance on substrate selection, storage, and handling as well as different test methods for quality testing of the adhesive bond between dental restorative materials and tooth structure, i.e. enamel and dentin.
This document does not include requirements for adhesive materials and their performance.
2 Normative references
The following documents contain requirements which, through reference in this text, constitute provisions of this document. For dated references, only the edition cited applies. For undated references, the latest edition (including any amendments) applies.
GB/T 6682-2008 Water for analytical laboratory use - Specification and test methods (ISO 3696:1987, MOD)
GB/T 9258.1-2000 Coated abrasives - Grain size analysis - Part 1: Grain size distribution test (idt ISO 6344-1:1998)
GB/T 9937 Dentistry - Vocabulary (GB/T 9937-2020, ISO 1942:2008, MOD)
YY 0302.1-2010 Dental rotary instruments - Burs - Part 1: Steel and carbide burs (ISO 3823-1:1997, MOD)
3 Terms and definitions
For the purposes of this document, the terms and definitions given in GB/T 9937 and the following apply.
3.1
adhere
to be in a state of adherence
3.2
adherence
state in which two surfaces are held together by interfacial forces
3.3
adherend
body that is held or is intended to be held to another body by an adhesive
3.4
adhesion
state in which two surfaces are held together by chemical or physical forces, or both, with the aid of an adhesive (3.5)
3.5
adhesive
substance capable of holding materials together
3.6
bond strength
force per unit area required to break a bonded assembly with failure occurring in or near the adhesive (3.5)/adherend interface
3.7
microleakage
passage of substances such as saliva, ions, compounds, or bacterial by-products between a cavity wall and the restorative material
3.8
substrate
material upon the surface of which an adhesive (3.5) is spread for bonding or coating
4 Sampling
The amount of test material shall be sufficient for all planned tests and be from the same batch.
Foreword i
Introduction iii
1 Scope
2 Normative references
3 Terms and definitions
4 Sampling
5 Test methods
Annex A (Informative) Test Methods for measurement of bond strength
Annex B (Informative) Test Method for tensile bond strength
Annex C (Informative) Test method for micro tensile bond strength
Annex D (Informative) Test method for shear bond strength (I)
Annex E (Informative) Test method for shear bond strength (II)
Bibliography
Dentistry - Testing of adhesion to tooth structure
1 Scope
This document specifies two bond strength measurements tests (tensile and shear), test for measurement of marginal gaps around fillings, a microleakage test, and some specific test methods for bond strength measurements.
This document gives guidance on substrate selection, storage, and handling as well as different test methods for quality testing of the adhesive bond between dental restorative materials and tooth structure, i.e. enamel and dentin.
This document does not include requirements for adhesive materials and their performance.
2 Normative references
The following documents contain requirements which, through reference in this text, constitute provisions of this document. For dated references, only the edition cited applies. For undated references, the latest edition (including any amendments) applies.
GB/T 6682-2008 Water for analytical laboratory use - Specification and test methods (ISO 3696:1987, MOD)
GB/T 9258.1-2000 Coated abrasives - Grain size analysis - Part 1: Grain size distribution test (idt ISO 6344-1:1998)
GB/T 9937 Dentistry - Vocabulary (GB/T 9937-2020, ISO 1942:2008, MOD)
YY 0302.1-2010 Dental rotary instruments - Burs - Part 1: Steel and carbide burs (ISO 3823-1:1997, MOD)
3 Terms and definitions
For the purposes of this document, the terms and definitions given in GB/T 9937 and the following apply.
3.1
adhere
to be in a state of adherence
3.2
adherence
state in which two surfaces are held together by interfacial forces
3.3
adherend
body that is held or is intended to be held to another body by an adhesive
3.4
adhesion
state in which two surfaces are held together by chemical or physical forces, or both, with the aid of an adhesive (3.5)
3.5
adhesive
substance capable of holding materials together
3.6
bond strength
force per unit area required to break a bonded assembly with failure occurring in or near the adhesive (3.5)/adherend interface
3.7
microleakage
passage of substances such as saliva, ions, compounds, or bacterial by-products between a cavity wall and the restorative material
3.8
substrate
material upon the surface of which an adhesive (3.5) is spread for bonding or coating
4 Sampling
The amount of test material shall be sufficient for all planned tests and be from the same batch.
Contents of YY/T 0519-2022
Foreword i
Introduction iii
1 Scope
2 Normative references
3 Terms and definitions
4 Sampling
5 Test methods
Annex A (Informative) Test Methods for measurement of bond strength
Annex B (Informative) Test Method for tensile bond strength
Annex C (Informative) Test method for micro tensile bond strength
Annex D (Informative) Test method for shear bond strength (I)
Annex E (Informative) Test method for shear bond strength (II)
Bibliography
