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GB 51205-2016   Code for design of PTA plant (English Version)
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Standard No.: GB 51205-2016
English Name: Code for design of PTA plant
Chinese Name: 精对苯二甲酸工厂设计规范
Professional Classification: GB    National Standard
Source Content Issued by: Ministry of Housing and Urban-Rural Construction of the People’s Republic of China
Issued on: 2016-10-25
Implemented on: 2017-7-1
Status: valid
Target Language: English
File Format: PDF
Word Count: 30000 words
Translation Price(USD): 750.0
Delivery: via email in 1 business day
Codeofchina.com is in charge of this English translation. In case of any doubt about the English translation, the Chinese original shall be considered authoritative. This code is formulated by China National Textile and Apparel Council and China Kunlun Contracting & Engineering Co. Ltd. jointly with organizations concerned according to the requirements of "Notice on Printing and Distributing the Development and Revision Plan of National Engineering Construction Standards and Codes in 2014" (JIANBIAO [2013] No.169) issued by the Ministry of Housing and Urban-Rural Development. During the formulation process, the code drafting group has carried out extensive investigation and study, summarized the construction experience of PTA plants in China over the years, especially the experience and lessons on design and construction of PTA plant with continuously expanding production scale and rapidly developing localized technology of PTA plant in recent years, and widely solicited for opinions on aspects such as production and construction, and then finalized this code through review. This code consists of 16 chapters and 1 annex, with specific technical contents covering: general provisions, terms, process design, process equipment, general layout design, equipment layout, process pipeline design, auxiliary production facilities, automatic control and instruments, electrical and telecommunication, building, structure, water supply and drainage, fire-fighting, occupational health and safety, environmental protection, etc. In this code, the provisions printed in bold type are mandatory and must be enforced strictly. The Ministry of Housing and Urban-Rural Development is in charge of the administration of this code and the explanation of the mandatory provisions, China National Textile and Apparel Council is responsible for routine management and China Kunlun Contracting & Engineering Co. Ltd. is responsible for the explanation of specific technical contents. All relevant organizations are kindly requested to carefully sum up experience in combination with engineering practices when implementing this code. The relevant modification and supplement, whenever necessary, should be fed back to China Kunlun Contracting & Engineering Co. Ltd. (address: No. 21 Zengguang Road, Haidian District, Beijing; 100037) for reference in future revision. Contents Foreword i 1 General Provisions 1 2 Terms 2 3 Process Design 4 3.1 General Requirements 4 3.2 Process Flow Design 5 3.3 Process Calculation 6 3.4 Hazard Factors 7 3.5 Safety Relief System 7 3.6 Insulation and Heat Tracing 8 4 Process Equipment 9 4.1 Equipment Type Selection 9 4.2 Equipment Material Selection 9 4.3 Equipment Structure Design 11 4.4 Selection of Equipment Design Parameter 11 4.5 Manufacture and Examination of Equipment 12 5 General Layout Design 15 6 Equipment Layout 17 6.1 Principles of Equipment Layout 17 6.2 Requirements of Equipment Layout 17 7 Process Pipeline Design 19 7.1 Pipeline Layout 19 7.2 Pipe Material Selection 19 7.3 Pipeline Flexibility Design 20 7.4 Pipeline Examination and Pressure Test 21 8 Auxiliary Production Facilities 23 8.1 Product Storehouse 23 8.2 Tank Farm 23 9 Automatic Control and Instruments 25 9.1 Automation Level 25 9.2 Main Control Strategies 25 9.3 Selection of Instruments and Control Valves 26 9.4 Control System Configuration 27 9.5 Control Room 28 9.6 Interlock Protection 29 9.7 Safety Measures for Instrument 30 10 Electrical and Telecommunication 32 10.1 General Requirements 32 10.2 Power Supply and Distribution 32 10.3 Lighting 34 10.4 Lightening Protection 35 10.5 Earthing 35 10.6 Automatic Fire Alarm System 36 10.7 Telecommunication 36 11 Building 37 11.1 General Requirements 37 11.2 Building Design 37 11.3 Fire, Explosion and Corrosion Prevention 38 12 Structure 40 12.1 General Requirements 40 12.2 Design Load 40 12.3 Structure Design 41 13 Water Supply and Drainage 44 13.1 Water Supply 44 13.2 Water Drainage 44 13.3 Pipeline of Water Supply and Drainage 45 14 Firefighting 47 15 Occupational Health and Safety 49 15.1 General Requirements 49 15.2 Fire and Explosion Prevention 49 15.3 Dust, Radiation Protection and Anticorrosive 49 15.4 Fall, Mechanical Injury Protection and Burn-proof Insulation 50 15.5 Safety Signs and Colors 50 15.6 Occupational Health Protection 51 15.7 Emergency Rescue 51 16 Environmental Protection 52 16.1 General Requirements 52 16.2 Waste Gas Treatment 52 16.3 Waste Water Treatment 52 16.4 Solid Waste Treatment 52 16.5 Noise Control 53 16.6 Measures for Prevention and Control of Water Pollution 53 Annex A Requirements of Explosion Hazards Classification for PTA Plant 55 Explanation of Wording in this Code 58 List of Quoted Standards 59 Code for Design of PTA Plant 1 General Provisions 1.0.1 This code is formulated with a view to unifying the technical requirements for design of PTA plant, improving the design level of PTA plant and realizing technical advancement, safety and environmental protection, energy conservation and consumption reduction, economy and rationality. 1.0.2 This code is applicable to the design of the newly-constructed, extended and reconstructed engineering, excluding the utilities and office facilities used for PTA plant. 1.0.3 The design of PTA plant shall not only meet the requirements stipulated in this code, but also comply with those in the current relevant ones of the nation. 2 Terms 2.0.1 plant for production of purified terephthalic acid (PTA plant) the plant producing acceptable industrial purified terephthalic acid products through oxidation reaction and purification reaction with p-xylene and air as raw materials. PTA plant is mainly composed of production device and auxiliary production facilities; the production device mainly includes oxidation unit and purification unit while the auxiliary production facilities mainly include product storehouse and tank farm 2.0.2 oxidation reaction the process generating crude terephthalic acid through reaction with p-xylene and air as raw materials, acetic acid as solvent, cobalt and manganese as catalyzer and bromine as accelerant 2.0.3 purification reaction the process of obtaining purified terephthalic acid through separation and drying after reducing the impurity carboxybenzaldehyde (4-CBA) in crude terephthalic acid to p-toluic acid (p-T acid) with crude terephthalic acid and hydrogen as raw materials and palladium/carbon as catalyzer 2.0.4 crude terephthalic acid (CTA) the product of oxidation unit, also the raw material of downstream purification unit 2.0.5 purified terephthalic acid (PTA) the product of purification unit, also the product of PTA plant 2.0.6 oxidation off gas the gas-phase product of oxidation reaction 2.0.7 entrainer the substance added during solvent recovery to form azeotrope with water, thereby separating the acetic acid and water mixture. Entrainer refers to common n-propyl acetate, n-butyl acetate or isobutyl acetate in this code 2.0.8 slurry the non-separated solid-liquid mixture containing CTA or PTA suspending particles 2.0.9 mother liquor the filtrate after slurry separation 2.0.10 pressure filtration the process realizing solid-liquid separation under certain positive pressure 2.0.11 drying the dehumidifying and drying process of wet filter cake after slurry filtration 3 Process Design 3.1 General Requirements 3.1.1 The process design of PTA plant shall meet the requirements of technical advancement, safety and reliability, energy conservation and environmental protection as well as economy and rationality. 3.1.2 The process design shall be based on the data of material balance and energy balance. 3.1.3 The comprehensive energy consumption index of newly-constructed, reconstructed or extended PTA plant shall meet the relevant requirements of the current national standard GB 31533 The Norm of Energy Consumption per Unit Product of Pure Terephthalic Acid. 3.1.4 The design annual operation time of PTA plant should be calculated as 8000h. 3.1.5 Washing facilities shall be arranged for the slurry pipeline between reactor and crystallizer. 3.1.6 Inert gas replacement facilities shall be arranged for the equipment and pipelines containing p-xylene, acetic acid, entrainer, methyl acetate and hydrogen. 3.1.7 Check valve shall be arranged at pump outlet pipeline delivering p-xylene, acetic acid, entrainer and methyl acetate. 3.1.8 Two drain valves shall be arranged at the low point of hydrogen pipeline; for the drain valves which may only be used at commencement and shutdown, a valve equipped with flange cover may be arranged. 3.1.9 The washing design of slurry pipeline shall meet the following requirements: 1 Check valve shall be arranged at the continuously used washing acid or process water pipeline, and block valve shall be arranged at the root of such pipeline. 2 Check valve and two block valves shall be arranged at the intermittently used washing acid, process water, alkali liquor and demineralized water pipelines, and drain valve shall be arranged at the low point between two block valves. 3 Blind plate or disconnection from the system shall be arranged for the alkali liquor pipeline used only upon equipment shutdown. 3.1.10 Isolating valve and 8-shaped blind plate shall be arranged for the pipeline delivering p-xylene, acetic acid, entrainer and hydrogen entering into the production device at the device boundary. 3.1.11 Metering instruments shall be arranged for various raw materials and utility media. 3.1.12 Sampling port shall be arranged respectively at the inlet and outlet pipelines of oxidation off gas purification system. 3.1.13 Sampling port shall be arranged at the exhaust funnel of oxidation off gas after purification treatment. The sampling port shall be of circular structure with nominal diameter of DN80~DN100. 3.1.14 Closed sampling shall be adopted for combustible liquids such as p-xylene, acetic acid, methyl acetate and entrainer. 3.1.15 Automatic sampler and manual sampling port should be simultaneously arranged on the pipeline delivering CTA and PTA powders. 3.2 Process Flow Design 3.2.1 The process flow shall be determined according to production scale, product scheme and product quality requirements. 3.2.2 The process flow shall meet the principles of advanced and mature technology, low material and energy consumption and less discharge of "three-waste". 3.2.3 The process flow design of oxidation unit shall meet the following requirements: 1 The oxidation off gas shall only be discharged after reaching the standard through purification and energy recovery; 2 The gas of atmospheric pressure system shall only be discharged after reaching the standard through purification treatment; 3 Pressure filtration process should be adopted for separation of CTA slurry; 4 Solvent recovery system shall be arranged, and the water separated by this system shall be recycled; 5 CTA, acetic acid, cobalt and manganese recovery system shall be arranged for the extracted oxidation mother liquor; 6 Oxidation mother liquor tank shall be arranged, and its capacity shall be able to contain the returned mother liquor of the system upon shutdown. 3.2.4 The process flow design of purification unit shall meet the following requirements: 1 Flash steam of crystallization system and its heat quantity shall be recycled; 2 A pass of pressure filtration process should be adopted; 3 Pneumatic conveying should be adopted for CTA and PTA powders; 4 PTA, cobalt and manganese recovery system shall be arranged for the purified mother liquor. 3.2.5 Slurry filter shall be arranged according to the processing capacity calculation of single equipment, and standby set shall be arranged based on the cleaning period and fault frequency of filter. 3.2.6 The steam system should be recycled according to the target temperature of the heated medium and the level of byproduct steam of device through level-by-level flashing of condensate. 3.2.7 The supply and return of the circulating cooling water shall be designed according to the resistance drop of equipment and pipeline and the difference of equipment installation height based on different pressures and systems. 3.3 Process Calculation 3.3.1 The whole process shall be subject to material balance and energy balance calculation. 3.3.2 The utility consumption of each equipment in production device shall be calculated. 3.3.3 The process calculation of non-stereotype equipment in production device shall be carried out according to logistic data and purpose. 3.3.4 Type selection of stereotype equipment in production device shall be determined according to the medium characteristic, operating parameter and arrangement quantity calculation. 3.3.5 The diameter and resistance drop of pipeline shall be determined through calculation, and should be implemented in accordance with the current professional standard SH/T 3035 Guide for Pipeline Sizing in Petrochemical Engineering. 3.3.6 The type selection of safety valve, rupture disk, breather valve, silencer and steam trap shall be determined according to the calculation based on different operating conditions. 3.3.7 The thermal insulation thickness of equipment and pipeline shall be determined through calculation.
Foreword i 1 General Provisions 2 Terms 3 Process Design 3.1 General Requirements 3.2 Process Flow Design 3.3 Process Calculation 3.4 Hazard Factors 3.5 Safety Relief System 3.6 Insulation and Heat Tracing 4 Process Equipment 4.1 Equipment Type Selection 4.2 Equipment Material Selection 4.3 Equipment Structure Design 4.4 Selection of Equipment Design Parameter 4.5 Manufacture and Examination of Equipment 5 General Layout Design 6 Equipment Layout 6.1 Principles of Equipment Layout 6.2 Requirements of Equipment Layout 7 Process Pipeline Design 7.1 Pipeline Layout 7.2 Pipe Material Selection 7.3 Pipeline Flexibility Design 7.4 Pipeline Examination and Pressure Test 8 Auxiliary Production Facilities 8.1 Product Storehouse 8.2 Tank Farm 9 Automatic Control and Instruments 9.1 Automation Level 9.2 Main Control Strategies 9.3 Selection of Instruments and Control Valves 9.4 Control System Configuration 9.5 Control Room 9.6 Interlock Protection 9.7 Safety Measures for Instrument 10 Electrical and Telecommunication 10.1 General Requirements 10.2 Power Supply and Distribution 10.3 Lighting 10.4 Lightening Protection 10.5 Earthing 10.6 Automatic Fire Alarm System 10.7 Telecommunication 11 Building 11.1 General Requirements 11.2 Building Design 11.3 Fire, Explosion and Corrosion Prevention 12 Structure 12.1 General Requirements 12.2 Design Load 12.3 Structure Design 13 Water Supply and Drainage 13.1 Water Supply 13.2 Water Drainage 13.3 Pipeline of Water Supply and Drainage 14 Firefighting 15 Occupational Health and Safety 15.1 General Requirements 15.2 Fire and Explosion Prevention 15.3 Dust, Radiation Protection and Anticorrosive 15.4 Fall, Mechanical Injury Protection and Burn-proof Insulation 15.5 Safety Signs and Colors 15.6 Occupational Health Protection 15.7 Emergency Rescue 16 Environmental Protection 16.1 General Requirements 16.2 Waste Gas Treatment 16.3 Waste Water Treatment 16.4 Solid Waste Treatment 16.5 Noise Control 16.6 Measures for Prevention and Control of Water Pollution Annex A Requirements of Explosion Hazards Classification for PTA Plant Explanation of Wording in this Code List of Quoted Standards
Referred in GB 51205-2016:
*GB 50009-2012 Load Code for the Design of Building Structures
*GB 50010-2010(2015) Code for design of concrete structures
*GB 50011-2010(2016) Code for Seismic Design of Buildings (2016)
*GB 50016-2014(2018)-Provisions Provisions of Code for Fire Protection Design of Buildings
*GB 50017-2017 Code for design of steel structures
*GB 50040-2020 Standard for design of dynamic machine foundation
*GB 50046-2008 Code for Anticorrosion Design of Industrial Constructions
*GB 50057-2010 Design Code for Protection of Structures against Lightning
*GB 50058-2014 Code for Design of Electrical Installations in Explosive Atmospheres
*GB 50074-2014 Code for design of oil depot
*GB 50116-2013 Code for design of automatic fire alarm system
*GB 50140-2005 Code for Design of Extinguisher Distribution in Buildings
*GB 50151-2021 Technical standard for foam extinguishing systems
*GB 50160-2008 Fire Prevention Code of Petrochemical Enterprise Design (Edition 2018)
*GB 50187-2012 Code for Design of General Layout of Industrial Enterprises
*GB 50191-2012 Design code for antiseismic of special structures
*GB 50223-2008 Standard for Classification of Seismic Protection of Building Cons
*GB 50343-2012 Technical code for protection of building electronic information system against lightning
*GB 50453-2008 Standard for classification of seismic protection of buildings and special structures in petrochemical engineering
*GB 50489-2009 Code for Design of General Plot Plan and Transportation of Chemical Industrial Enterprises
*GB 50493-2009 Specification for Design of Combustible Gas and Toxic Gas Detection and Alarm for Petrochemical Industry
*GB 50517-2010 Code for Construction Quality Acceptance of Metallic Piping in Petrochemical Engineering
*GB 50650-2011(2022) Code for design protection of petrochemical plant against lightning
*GB/T 50770-2013 Code for design of safety instrumented system in petrochemical engineering
*GB 50779-2012 Code for design of blast resistant control building in petrochemical industry
*GB 50868-2013 Standard for allowable vibration of building engineering
*GB/T 50934-2013 Technical Code for Seepage Prevention in Petrochemical Engineering
*GB 50974-2014 Code of design on fire protection water supply and hydrant systems
*GB 51006-2014 Load code for design of buildings and special structures in petrochemical industry
*GB/T 51082-2015 Code for coating design of industrial constructions
*GBT150.4-
*GB 2893-2008 Safety colours
*GB 2894-2008 Safety Signs and Guideline for the Use
*GB4053-
*GB/T 4334-2020 Corrosion of metals and alloys—Test methods for intergranular corrosion of austenitic and ferritic-austenitic (duplex) stainless steels
*GB/T 5310-2023 Seamless steel tubes and pipes for high pressure boiler
*GBT6479-
*GB 7231-2003 Basic indentification colors and code indications and safety sign for industrial pipelines
*GB/T 11651-2008 Code of practice for selection of personal protective equipments
*GB 12348-2008 Emission Standard for Industrial Enterprises Noise at Boundary
*GB 18597-2023 Standard for pollution control on hazardous waste storage
*GB 18599-2020 Standard for pollution control on the non-hazardous industrial solid waste storage and landfill
*GBT21109-
*GB 31533-2015 The norm of energy consumption per unit product of pure terephthalic acid
*GB 31571-2015 Emission standard of pollutants for petroleum chemistry industry
*GBZ 1-2010 Hygienic Standards for the Design of Industrial Enterprises
*GBZ 125-2009 Radiological protection requirements for gauges containing sealed radioactive source
*GBZ 158-2003 Warning Signs for Occupational Hazards in the Workplace
*AQ/T 3049-2013 Hazard and Operability Studies(HAZOP Studies) - Application Guide
*GA 1002-2012 Public security protection requirements for hypertoxic chemicals and radioactive sources storage site
*JB/T 4745-2002 Titanium welded vessels
*NB/T47002.1-47002.4-2009
*NB/T 47002.3-2019 Clad plate for pressure vessel - Part 3: Titanium-steel clad plate
*NBT47013-
*SH/T 3006-2024 Design specification for control roomin petrochemical industry
*SH/T 3007-2014 Specification for Design of Tank Farms for Petrochemical Storage
*SH/T 3010-2013 Design code for insulation engineering of petrochemical equipment and pipe
*SH/T 3035-2018 Guideline for pipeline sizing in petrochemical industry
*SH/T 3081-2019 Design code for instrument earthing in petrochemical industry
*SH/T 3137-2013 Technical specification of fire protection for steel structures in petrochemical industry
*SH 3147-2014 Code for seismic design of special structures for petrochemical
*SH/T 3164-2021 Design specification for instrument system lightning surge protection in petrochemical industry
*SH/T 3421-2009 General rules for arrangement and selection of metal bellows expansion joint
*SH 3501-2011 Construction and acceptance Specification for toxic and combustible medium steel piping engineering in petrochemical industry
GB 51205-2016 is referred in:
*GB 5009.236-2016 National Food Safety Standard - Animal and Vegetable Fats and Oils - Determination of Moisture and Volatile Matter
*GB 5009.228-2016 National Food Safety Standard - Determination of Volatile Basic Nitrogen in Food
*GB 31604.6-2016 National Food Safety Standard - Food Contact Materials and Articles -Determination of Ignition Residue in Resin
*GB 1886.26-2016 National Food Safety Standard - Food Additives - Paraffin
*GB 1886.187-2016 National Food Safety Standard - Food Additives - Sorbitol and Sorbitol Solution
*GB 1886.169-2016 National Food Safety Standard - Food Additives - Carrageenan
*GB 5413.38-2016 National Food Safety Standard - Determination of freezing point in raw milk in food
*GB 51173-2016 Code for design of dewatering and draining in opne pit mine of coal industry
*GB 51199-2016 Code for acceptance of construction engineering of telecommunication power supply facility
Code of China
Standard
GB 51205-2016  Code for design of PTA plant (English Version)
Standard No.GB 51205-2016
Statusvalid
LanguageEnglish
File FormatPDF
Word Count30000 words
Price(USD)750.0
Implemented on2017-7-1
Deliveryvia email in 1 business day
Detail of GB 51205-2016
Standard No.
GB 51205-2016
English Name
Code for design of PTA plant
Chinese Name
精对苯二甲酸工厂设计规范
Chinese Classification
Professional Classification
GB
ICS Classification
Issued by
Ministry of Housing and Urban-Rural Construction of the People’s Republic of China
Issued on
2016-10-25
Implemented on
2017-7-1
Status
valid
Superseded by
Superseded on
Abolished on
Superseding
Language
English
File Format
PDF
Word Count
30000 words
Price(USD)
750.0
Keywords
GB 51205-2016, GB/T 51205-2016, GBT 51205-2016, GB51205-2016, GB 51205, GB51205, GB/T51205-2016, GB/T 51205, GB/T51205, GBT51205-2016, GBT 51205, GBT51205
Introduction of GB 51205-2016
Codeofchina.com is in charge of this English translation. In case of any doubt about the English translation, the Chinese original shall be considered authoritative. This code is formulated by China National Textile and Apparel Council and China Kunlun Contracting & Engineering Co. Ltd. jointly with organizations concerned according to the requirements of "Notice on Printing and Distributing the Development and Revision Plan of National Engineering Construction Standards and Codes in 2014" (JIANBIAO [2013] No.169) issued by the Ministry of Housing and Urban-Rural Development. During the formulation process, the code drafting group has carried out extensive investigation and study, summarized the construction experience of PTA plants in China over the years, especially the experience and lessons on design and construction of PTA plant with continuously expanding production scale and rapidly developing localized technology of PTA plant in recent years, and widely solicited for opinions on aspects such as production and construction, and then finalized this code through review. This code consists of 16 chapters and 1 annex, with specific technical contents covering: general provisions, terms, process design, process equipment, general layout design, equipment layout, process pipeline design, auxiliary production facilities, automatic control and instruments, electrical and telecommunication, building, structure, water supply and drainage, fire-fighting, occupational health and safety, environmental protection, etc. In this code, the provisions printed in bold type are mandatory and must be enforced strictly. The Ministry of Housing and Urban-Rural Development is in charge of the administration of this code and the explanation of the mandatory provisions, China National Textile and Apparel Council is responsible for routine management and China Kunlun Contracting & Engineering Co. Ltd. is responsible for the explanation of specific technical contents. All relevant organizations are kindly requested to carefully sum up experience in combination with engineering practices when implementing this code. The relevant modification and supplement, whenever necessary, should be fed back to China Kunlun Contracting & Engineering Co. Ltd. (address: No. 21 Zengguang Road, Haidian District, Beijing; 100037) for reference in future revision. Contents Foreword i 1 General Provisions 1 2 Terms 2 3 Process Design 4 3.1 General Requirements 4 3.2 Process Flow Design 5 3.3 Process Calculation 6 3.4 Hazard Factors 7 3.5 Safety Relief System 7 3.6 Insulation and Heat Tracing 8 4 Process Equipment 9 4.1 Equipment Type Selection 9 4.2 Equipment Material Selection 9 4.3 Equipment Structure Design 11 4.4 Selection of Equipment Design Parameter 11 4.5 Manufacture and Examination of Equipment 12 5 General Layout Design 15 6 Equipment Layout 17 6.1 Principles of Equipment Layout 17 6.2 Requirements of Equipment Layout 17 7 Process Pipeline Design 19 7.1 Pipeline Layout 19 7.2 Pipe Material Selection 19 7.3 Pipeline Flexibility Design 20 7.4 Pipeline Examination and Pressure Test 21 8 Auxiliary Production Facilities 23 8.1 Product Storehouse 23 8.2 Tank Farm 23 9 Automatic Control and Instruments 25 9.1 Automation Level 25 9.2 Main Control Strategies 25 9.3 Selection of Instruments and Control Valves 26 9.4 Control System Configuration 27 9.5 Control Room 28 9.6 Interlock Protection 29 9.7 Safety Measures for Instrument 30 10 Electrical and Telecommunication 32 10.1 General Requirements 32 10.2 Power Supply and Distribution 32 10.3 Lighting 34 10.4 Lightening Protection 35 10.5 Earthing 35 10.6 Automatic Fire Alarm System 36 10.7 Telecommunication 36 11 Building 37 11.1 General Requirements 37 11.2 Building Design 37 11.3 Fire, Explosion and Corrosion Prevention 38 12 Structure 40 12.1 General Requirements 40 12.2 Design Load 40 12.3 Structure Design 41 13 Water Supply and Drainage 44 13.1 Water Supply 44 13.2 Water Drainage 44 13.3 Pipeline of Water Supply and Drainage 45 14 Firefighting 47 15 Occupational Health and Safety 49 15.1 General Requirements 49 15.2 Fire and Explosion Prevention 49 15.3 Dust, Radiation Protection and Anticorrosive 49 15.4 Fall, Mechanical Injury Protection and Burn-proof Insulation 50 15.5 Safety Signs and Colors 50 15.6 Occupational Health Protection 51 15.7 Emergency Rescue 51 16 Environmental Protection 52 16.1 General Requirements 52 16.2 Waste Gas Treatment 52 16.3 Waste Water Treatment 52 16.4 Solid Waste Treatment 52 16.5 Noise Control 53 16.6 Measures for Prevention and Control of Water Pollution 53 Annex A Requirements of Explosion Hazards Classification for PTA Plant 55 Explanation of Wording in this Code 58 List of Quoted Standards 59 Code for Design of PTA Plant 1 General Provisions 1.0.1 This code is formulated with a view to unifying the technical requirements for design of PTA plant, improving the design level of PTA plant and realizing technical advancement, safety and environmental protection, energy conservation and consumption reduction, economy and rationality. 1.0.2 This code is applicable to the design of the newly-constructed, extended and reconstructed engineering, excluding the utilities and office facilities used for PTA plant. 1.0.3 The design of PTA plant shall not only meet the requirements stipulated in this code, but also comply with those in the current relevant ones of the nation. 2 Terms 2.0.1 plant for production of purified terephthalic acid (PTA plant) the plant producing acceptable industrial purified terephthalic acid products through oxidation reaction and purification reaction with p-xylene and air as raw materials. PTA plant is mainly composed of production device and auxiliary production facilities; the production device mainly includes oxidation unit and purification unit while the auxiliary production facilities mainly include product storehouse and tank farm 2.0.2 oxidation reaction the process generating crude terephthalic acid through reaction with p-xylene and air as raw materials, acetic acid as solvent, cobalt and manganese as catalyzer and bromine as accelerant 2.0.3 purification reaction the process of obtaining purified terephthalic acid through separation and drying after reducing the impurity carboxybenzaldehyde (4-CBA) in crude terephthalic acid to p-toluic acid (p-T acid) with crude terephthalic acid and hydrogen as raw materials and palladium/carbon as catalyzer 2.0.4 crude terephthalic acid (CTA) the product of oxidation unit, also the raw material of downstream purification unit 2.0.5 purified terephthalic acid (PTA) the product of purification unit, also the product of PTA plant 2.0.6 oxidation off gas the gas-phase product of oxidation reaction 2.0.7 entrainer the substance added during solvent recovery to form azeotrope with water, thereby separating the acetic acid and water mixture. Entrainer refers to common n-propyl acetate, n-butyl acetate or isobutyl acetate in this code 2.0.8 slurry the non-separated solid-liquid mixture containing CTA or PTA suspending particles 2.0.9 mother liquor the filtrate after slurry separation 2.0.10 pressure filtration the process realizing solid-liquid separation under certain positive pressure 2.0.11 drying the dehumidifying and drying process of wet filter cake after slurry filtration 3 Process Design 3.1 General Requirements 3.1.1 The process design of PTA plant shall meet the requirements of technical advancement, safety and reliability, energy conservation and environmental protection as well as economy and rationality. 3.1.2 The process design shall be based on the data of material balance and energy balance. 3.1.3 The comprehensive energy consumption index of newly-constructed, reconstructed or extended PTA plant shall meet the relevant requirements of the current national standard GB 31533 The Norm of Energy Consumption per Unit Product of Pure Terephthalic Acid. 3.1.4 The design annual operation time of PTA plant should be calculated as 8000h. 3.1.5 Washing facilities shall be arranged for the slurry pipeline between reactor and crystallizer. 3.1.6 Inert gas replacement facilities shall be arranged for the equipment and pipelines containing p-xylene, acetic acid, entrainer, methyl acetate and hydrogen. 3.1.7 Check valve shall be arranged at pump outlet pipeline delivering p-xylene, acetic acid, entrainer and methyl acetate. 3.1.8 Two drain valves shall be arranged at the low point of hydrogen pipeline; for the drain valves which may only be used at commencement and shutdown, a valve equipped with flange cover may be arranged. 3.1.9 The washing design of slurry pipeline shall meet the following requirements: 1 Check valve shall be arranged at the continuously used washing acid or process water pipeline, and block valve shall be arranged at the root of such pipeline. 2 Check valve and two block valves shall be arranged at the intermittently used washing acid, process water, alkali liquor and demineralized water pipelines, and drain valve shall be arranged at the low point between two block valves. 3 Blind plate or disconnection from the system shall be arranged for the alkali liquor pipeline used only upon equipment shutdown. 3.1.10 Isolating valve and 8-shaped blind plate shall be arranged for the pipeline delivering p-xylene, acetic acid, entrainer and hydrogen entering into the production device at the device boundary. 3.1.11 Metering instruments shall be arranged for various raw materials and utility media. 3.1.12 Sampling port shall be arranged respectively at the inlet and outlet pipelines of oxidation off gas purification system. 3.1.13 Sampling port shall be arranged at the exhaust funnel of oxidation off gas after purification treatment. The sampling port shall be of circular structure with nominal diameter of DN80~DN100. 3.1.14 Closed sampling shall be adopted for combustible liquids such as p-xylene, acetic acid, methyl acetate and entrainer. 3.1.15 Automatic sampler and manual sampling port should be simultaneously arranged on the pipeline delivering CTA and PTA powders. 3.2 Process Flow Design 3.2.1 The process flow shall be determined according to production scale, product scheme and product quality requirements. 3.2.2 The process flow shall meet the principles of advanced and mature technology, low material and energy consumption and less discharge of "three-waste". 3.2.3 The process flow design of oxidation unit shall meet the following requirements: 1 The oxidation off gas shall only be discharged after reaching the standard through purification and energy recovery; 2 The gas of atmospheric pressure system shall only be discharged after reaching the standard through purification treatment; 3 Pressure filtration process should be adopted for separation of CTA slurry; 4 Solvent recovery system shall be arranged, and the water separated by this system shall be recycled; 5 CTA, acetic acid, cobalt and manganese recovery system shall be arranged for the extracted oxidation mother liquor; 6 Oxidation mother liquor tank shall be arranged, and its capacity shall be able to contain the returned mother liquor of the system upon shutdown. 3.2.4 The process flow design of purification unit shall meet the following requirements: 1 Flash steam of crystallization system and its heat quantity shall be recycled; 2 A pass of pressure filtration process should be adopted; 3 Pneumatic conveying should be adopted for CTA and PTA powders; 4 PTA, cobalt and manganese recovery system shall be arranged for the purified mother liquor. 3.2.5 Slurry filter shall be arranged according to the processing capacity calculation of single equipment, and standby set shall be arranged based on the cleaning period and fault frequency of filter. 3.2.6 The steam system should be recycled according to the target temperature of the heated medium and the level of byproduct steam of device through level-by-level flashing of condensate. 3.2.7 The supply and return of the circulating cooling water shall be designed according to the resistance drop of equipment and pipeline and the difference of equipment installation height based on different pressures and systems. 3.3 Process Calculation 3.3.1 The whole process shall be subject to material balance and energy balance calculation. 3.3.2 The utility consumption of each equipment in production device shall be calculated. 3.3.3 The process calculation of non-stereotype equipment in production device shall be carried out according to logistic data and purpose. 3.3.4 Type selection of stereotype equipment in production device shall be determined according to the medium characteristic, operating parameter and arrangement quantity calculation. 3.3.5 The diameter and resistance drop of pipeline shall be determined through calculation, and should be implemented in accordance with the current professional standard SH/T 3035 Guide for Pipeline Sizing in Petrochemical Engineering. 3.3.6 The type selection of safety valve, rupture disk, breather valve, silencer and steam trap shall be determined according to the calculation based on different operating conditions. 3.3.7 The thermal insulation thickness of equipment and pipeline shall be determined through calculation.
Contents of GB 51205-2016
Foreword i 1 General Provisions 2 Terms 3 Process Design 3.1 General Requirements 3.2 Process Flow Design 3.3 Process Calculation 3.4 Hazard Factors 3.5 Safety Relief System 3.6 Insulation and Heat Tracing 4 Process Equipment 4.1 Equipment Type Selection 4.2 Equipment Material Selection 4.3 Equipment Structure Design 4.4 Selection of Equipment Design Parameter 4.5 Manufacture and Examination of Equipment 5 General Layout Design 6 Equipment Layout 6.1 Principles of Equipment Layout 6.2 Requirements of Equipment Layout 7 Process Pipeline Design 7.1 Pipeline Layout 7.2 Pipe Material Selection 7.3 Pipeline Flexibility Design 7.4 Pipeline Examination and Pressure Test 8 Auxiliary Production Facilities 8.1 Product Storehouse 8.2 Tank Farm 9 Automatic Control and Instruments 9.1 Automation Level 9.2 Main Control Strategies 9.3 Selection of Instruments and Control Valves 9.4 Control System Configuration 9.5 Control Room 9.6 Interlock Protection 9.7 Safety Measures for Instrument 10 Electrical and Telecommunication 10.1 General Requirements 10.2 Power Supply and Distribution 10.3 Lighting 10.4 Lightening Protection 10.5 Earthing 10.6 Automatic Fire Alarm System 10.7 Telecommunication 11 Building 11.1 General Requirements 11.2 Building Design 11.3 Fire, Explosion and Corrosion Prevention 12 Structure 12.1 General Requirements 12.2 Design Load 12.3 Structure Design 13 Water Supply and Drainage 13.1 Water Supply 13.2 Water Drainage 13.3 Pipeline of Water Supply and Drainage 14 Firefighting 15 Occupational Health and Safety 15.1 General Requirements 15.2 Fire and Explosion Prevention 15.3 Dust, Radiation Protection and Anticorrosive 15.4 Fall, Mechanical Injury Protection and Burn-proof Insulation 15.5 Safety Signs and Colors 15.6 Occupational Health Protection 15.7 Emergency Rescue 16 Environmental Protection 16.1 General Requirements 16.2 Waste Gas Treatment 16.3 Waste Water Treatment 16.4 Solid Waste Treatment 16.5 Noise Control 16.6 Measures for Prevention and Control of Water Pollution Annex A Requirements of Explosion Hazards Classification for PTA Plant Explanation of Wording in this Code List of Quoted Standards
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Keywords:
GB 51205-2016, GB/T 51205-2016, GBT 51205-2016, GB51205-2016, GB 51205, GB51205, GB/T51205-2016, GB/T 51205, GB/T51205, GBT51205-2016, GBT 51205, GBT51205